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MPMS3 Squid®

MPMS3

Quantum Design's Magnetic Property Measurement System (MPMS) is a suite of analytical instruments designed to study the magnetic properties of experimental samples. Measurements can be automated and performed across a range of temperature and magnetic field strengths. Although this and the DynaCool™ share some functional overlap the MPMS instrument can obtain higher resolution measurements using a Superconducting Quantum Interference Device (SQUID) in combination with superconducting pickup coils. The system is also capable of much faster field charging and temperature cooling rates.

Measurements:

Experimental samples are first mounted and centered in a magnetically neutral medium. High quality materials, such as quartz tubing, are available but these are often brittle or fragile. For less sensitive measurements a more robust approach utilizes drinking straws that have been tested for magnetic impurities. Once mounted the sample holder is sealed and connected to a rod before being lowered into the sample probe.

How it works:

When a measurement begins the linear transport motor, which sits atop the sample probe, begins driving the sample up and down through a region of the chamber surrounded by super conducting coils. As a magnetic sample moves up and down through the detection coils it creates magnetic flux and induces an electrical current. The detection coils form a closed loop with the SQUID component. The induction of a current across this closed circuit, in response to the sample, is proportional to the magnetic flux.

The SQUID's Role

The SQUID functions as a highly linear current-to-voltage convertor through the use of two parallel Josephson junctions separated by thin insulating layers. The device itself built on a small chip and seated at the bottom of the sample probe. This circuit is highly sensitive to magnetic field fluctuations and must be heavily shielded to reduce noise.

Specifications:

Temperature Control:  
Range: 1.8 to 400 K Standard; 1.8 to 1000 K with Oven option
Cooling Rate: 30 K/min (300 to 10 K in 15 minutes)
  10 K/min (10 to 1.8 K in 5 minutes)
Magnet Control:  
Range: -70 kOe to +70 kOe
Charging Rate: 4 Oe/sec to 700 Oe/sec
Uniformity: ±0.01% over 4 cm on axis
Charging Resolution: 0.33 Oe
Measurements:  
Maximum DC moment: 10 emu
Sensitivity
(≤ 2,500 Oe):
≤ 5 x 10-8 emu (DC scan)
  ≤ 1 x 10-8 emu (VSM, less than 10 second averaging)*
Sensitivity
(> 2,500 Oe):
≤ 6 x 10-7 emu (DC scan)
  ≤ 8 x 10-8 emu (VSM, less than 10 second averaging)*
Variable drive amplitude: 0.1 to 8 mm (peak)
General Details:  
Measurement Options: VSM EverCool, VSM Oven (1000 K), AC option
Sample Chamber Size: Inner Diameter of 9 mm

Related research publications using this instrument

 

Lab: 

Location: 

The SQUID MPMS3 instrument is located in the Low-Temperature Lab, Room 1055, at the Materials Research Lab

Manufacturer's Info: 

The manufacturer's description is posted at https://qdusa.com/products/mpms3.html

Instrument Information and/or Manual: 

Contact: 

To request training or inquire about sending samples please contact amanda [at] mrl [dot] ucsb [dot] edu (Amanda Strom) or seshadri [at] mrl [dot] ucsb [dot] edu (Ram Seshadri).