Quantum Design's Magnetic Property Measurement System (MPMS) is a suite of analytical instruments designed to study the magnetic properties of experimental samples. Measurements can be automated and performed across a range of temperature and magnetic field strengths. Although this and the DynaCool™ share some functional overlap the MPMS instrument can obtain higher resolution measurements using a Superconducting Quantum Interference Device (SQUID) in combination with superconducting pickup coils. The system is also capable of much faster field charging and temperature cooling rates.
Measurements:
Experimental samples are first mounted and centered in a magnetically neutral medium. High quality materials, such as quartz tubing, are available but these are often brittle or fragile. For less sensitive measurements a more robust approach utilizes drinking straws that have been tested for magnetic impurities. Once mounted the sample holder is sealed and connected to a rod before being lowered into the sample probe.
How it works:
When a measurement begins the linear transport motor, which sits atop the sample probe, begins driving the sample up and down through a region of the chamber surrounded by super conducting coils. As a magnetic sample moves up and down through the detection coils it creates magnetic flux and induces an electrical current. The detection coils form a closed loop with the SQUID component. The induction of a current across this closed circuit, in response to the sample, is proportional to the magnetic flux.
The SQUID's Role
The SQUID functions as a highly linear current-to-voltage convertor through the use of two parallel Josephson junctions separated by thin insulating layers. The device itself built on a small chip and seated at the bottom of the sample probe. This circuit is highly sensitive to magnetic field fluctuations and must be heavily shielded to reduce noise.
Specifications:
Temperature Control: | |
---|---|
Range: | 1.8 to 400 K Standard; 1.8 to 1000 K with Oven option |
Cooling Rate: | 30 K/min (300 to 10 K in 15 minutes) |
10 K/min (10 to 1.8 K in 5 minutes) | |
Magnet Control: | |
Range: | -70 kOe to +70 kOe |
Charging Rate: | 4 Oe/sec to 700 Oe/sec |
Uniformity: | ±0.01% over 4 cm on axis |
Charging Resolution: | 0.33 Oe |
Measurements: | |
Maximum DC moment: | 10 emu |
Sensitivity (≤ 2,500 Oe): |
≤ 5 x 10-8 emu (DC scan) |
≤ 1 x 10-8 emu (VSM, less than 10 second averaging)* | |
Sensitivity (> 2,500 Oe): |
≤ 6 x 10-7 emu (DC scan) |
≤ 8 x 10-8 emu (VSM, less than 10 second averaging)* | |
Variable drive amplitude: | 0.1 to 8 mm (peak) |
General Details: | |
Measurement Options: | VSM EverCool, VSM Oven (1000 K), AC option |
Sample Chamber Size: | Inner Diameter of 9 mm |
Related research publications using this instrument
- Deciphering structural and magnetic disorder in the chiral skyrmion host materials CoxZnyMnz (x+y+z=20)
- High-Pressure Laser Floating Zone Furnace
- Low magnetic damping and large negative anisotropic magnetoresistance in half-metallic Co2-xMn1+xSi Heusler alloy films grown by molecular beam epitaxy
Lab:
Location:
The SQUID MPMS3 instrument is located in the Low-Temperature Lab, Room 1055, at the Materials Research Lab
Manufacturer's Info:
The manufacturer's description is posted at https://qdusa.com/products/mpms3.html
Instrument Information and/or Manual:
Attachment | Size |
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MPMS3 Users Manual | 6.44 MB |
VSM AC Option Manual | 3.47 MB |
VSM Oven Option Manual | 882.89 KB |
High Temperature AC Measurement Applications Notes | 303.86 KB |
Fundamentals of Magnetism for MPMS | 8.55 MB |
Contact:
To request training or inquire about sending samples please contact amanda [at] mrl [dot] ucsb [dot] edu (Amanda Strom) or seshadri [at] mrl [dot] ucsb [dot] edu (Ram Seshadri).